Journal Description
Minerals
Minerals
is an international, peer-reviewed, open access journal of natural mineral systems, mineral resources, mining, and mineral processing. Minerals is published monthly online by MDPI.
- Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
- High Visibility: indexed within Scopus, SCIE (Web of Science), GeoRef, CaPlus / SciFinder, Inspec, Astrophysics Data System, AGRIS, and other databases.
- Journal Rank: JCR - Q2 (Mining & Mineral Processing) / CiteScore - Q2 (Geology)
- Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 18.7 days after submission; acceptance to publication is undertaken in 2.6 days (median values for papers published in this journal in the second half of 2023).
- Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
- Companion journal: Mining
Impact Factor:
2.5 (2022);
5-Year Impact Factor:
2.7 (2022)
Latest Articles
Experimental Investigation on Hydrophobic Alteration of Mining Solid Waste Backfill Material
Minerals 2024, 14(6), 580; https://doi.org/10.3390/min14060580 (registering DOI) - 30 May 2024
Abstract
Abstract: To address the issues of corrosion weakening of solid-waste-based backfill material caused by mine water, a novel hydrophobic solid waste backfill (HSBF) material was developed using polydimethylsiloxane (PDMS) and a silane coupling agent (SCA) as hydrophobic modification additives, and NaOH (SH) and
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Abstract: To address the issues of corrosion weakening of solid-waste-based backfill material caused by mine water, a novel hydrophobic solid waste backfill (HSBF) material was developed using polydimethylsiloxane (PDMS) and a silane coupling agent (SCA) as hydrophobic modification additives, and NaOH (SH) and sodium silicate (SS) as alkali activators. Fly ash and slag were chosen as the primary raw solid waste materials. The rheological properties of the hydrophobic-treated backfill slurries were measured, and the resulting physicochemical properties were compared with the unmodified reference group. This study reveals that the fresh HSBF slurry follows a Modified Bingham (M-B) model with shear-thinning characteristics. The addition of PDMS causes an increase in the water contact angle of the hardened HSBF material with F8S2 to up to 134.9°, indicating high hydrophobicity. Morphological observations indicated that PDMS mainly attaches to the inorganic particles’ surface through the bridging action of SCA for the hydrophobic modification of the backfill material. The overall strength of the HSBF materials was further ensured via fly ash–slag ratio optimization, and was found to be enhanced up to 98% by increasing slag content from 20% to 50%. This is mainly attributed to the hydration of slag, forming C-S(A)-H gel, which contributes to the increased strength. The novel HSBF material enables the elimination of cement in mine backfilling applications, demonstrating good economic benefits. Its excellent mechanical and hydrophobic properties can not only prevent overburden displacement in goaf areas, but can also mitigate water resource loss from overlying strata and simultaneously reduce the safety risks associated with long-term mine water deterioration.
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(This article belongs to the Special Issue Cemented Mine Waste Backfill: Experiment and Modelling: 2nd Edition)
Open AccessArticle
Adsorption Characteristics of Illite and Kerogen Oil Phase: Thermodynamics Experiments
by
Xin Tang, Junjie Xiong, Yanming Zhu, Ruiyu He, Xiangru Chen, Qiuqi Chen, Zhangping Yan, Cheng Liu and Litao Ma
Minerals 2024, 14(6), 579; https://doi.org/10.3390/min14060579 (registering DOI) - 30 May 2024
Abstract
In order to study the adsorption process and adsorption characteristics of shale oil at the macro scale, the isothermal adsorption experiments of illite and kerogen on a heptadecane (oil phase) solution were carried out by infrared spectrophotometry and gas chromatography–mass spectrometry. Based on
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In order to study the adsorption process and adsorption characteristics of shale oil at the macro scale, the isothermal adsorption experiments of illite and kerogen on a heptadecane (oil phase) solution were carried out by infrared spectrophotometry and gas chromatography–mass spectrometry. Based on the adsorption isotherm model and adsorption thermodynamic model, the characteristics of heptadecane adsorbed by illite and kerogen at different temperatures and oily solution concentrations were studied. The experimental results show that the concentration and temperature of the alkane solution help to enhance the adsorption and increase the saturated adsorption capacity. The difference is that the concentration will have a certain effect on the adsorption rate, while the temperature will not. Based on the three adsorption isotherm models, it was found that Langmuir and Freundlich were more suitable for describing the adsorption process of the heptadecane solution by illite and kerogen, and the adsorption characteristics of heptadecane molecules at different temperatures and adsorbents were evaluated. Heating leads to an increase in the collision efficiency between adsorbate molecules and adsorbents, thereby accelerating the migration rate of alkanes. Therefore, increasing temperature helps to enhance the adsorption capacity of rocks and increase the saturated adsorption capacity of minerals. The research results clarify the adsorption characteristics of shale oil heavy components from the macro level and fill the research gap in the application of solid–liquid isothermal adsorption physical experiments on the adsorption and occurrence of shale oil.
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(This article belongs to the Section Clays and Engineered Mineral Materials)
Open AccessArticle
U-Pb LA-ICP-MS Zircon Dating of Crustal Xenoliths: Evidence of the Archean Lithosphere Beneath the Snake River Plain
by
William P. Leeman, Jeffrey D. Vervoort and S. Andrew DuFrane
Minerals 2024, 14(6), 578; https://doi.org/10.3390/min14060578 - 30 May 2024
Abstract
New U-Pb zircon ages are reported for granulite facies crustal xenoliths brought to the surface by mafic lavas in the Snake River Plain. All samples yield Meso-to-Neoarchean ages (2.4–3.6 Ga) that significantly expand the known extent of the Archean Wyoming Craton at least
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New U-Pb zircon ages are reported for granulite facies crustal xenoliths brought to the surface by mafic lavas in the Snake River Plain. All samples yield Meso-to-Neoarchean ages (2.4–3.6 Ga) that significantly expand the known extent of the Archean Wyoming Craton at least as far west as the west-central Snake River Plain. Most zircon populations indicate multiple growth episodes with complexity increasing eastward, but they bear no record of major Phanerozoic magmatic episodes in the region. To extrapolate this work further west to the inferred craton boundary, zircons from southwestern Idaho batholith granodiorites were also analyzed. Although most batholith zircons record Cretaceous formation ages, all samples have zircons with inherited cores—with some recording Proterozoic ages (approaching 2 Ga). These data enhance our perspectives regarding lithosphere architecture beneath southern Idaho and adjacent areas and its possible influence on Cenozoic magmatism associated with the Snake River Plain–Yellowstone “melting anomaly”.
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(This article belongs to the Section Mineral Geochemistry and Geochronology)
Open AccessArticle
The Microdeformation Fabric of Amphibole-Rich Peridotite in the Southern Mariana Trench and Its Influence on Seismic Anisotropy
by
Jingbo Li and Zhenmin Jin
Minerals 2024, 14(6), 577; https://doi.org/10.3390/min14060577 - 30 May 2024
Abstract
Olivine, the most abundant mineral in the upper mantle, exhibits elastic anisotropy. Understanding the seismic anisotropy and flow patterns in the upper mantle hinges on the crystallographic preferred orientation (CPO) of olivine. Similarly, hydrous minerals, which also display elastic anisotropy, play a crucial
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Olivine, the most abundant mineral in the upper mantle, exhibits elastic anisotropy. Understanding the seismic anisotropy and flow patterns in the upper mantle hinges on the crystallographic preferred orientation (CPO) of olivine. Similarly, hydrous minerals, which also display elastic anisotropy, play a crucial role in explaining seismic anisotropy in numerous subduction zones. High-temperature and -pressure simple shear experiments reveal that the CPO of amphibole can lead to significant seismic anisotropy. In this study, peridotite samples originating from the southern end of the Mariana Trench, commonly containing amphibole, were analyzed. The microdeformation fabric and seismic anisotropy were examined. The results indicate a weak fabric strength in olivine, yet identifiable deformation fabrics of A/D, D, and AG were observed. Various dislocation structures suggest that olivine experiences complex deformation across various temperatures. Not only can the original slip system transform, but the melt/fluid resulting from melting also has a substantial impact on the peridotite. Deformation precedes the melt/rock interaction, resulting in a strong melt/rock reaction under near-static conditions. Furthermore, the modal content of amphibole significantly alters the seismic anisotropy of peridotite. An increase in amphibole content (types I, III, and IV) enhances seismic anisotropy, particularly for type I amphibole. Notably, the presence of type I fabric amphibole promotes the Vs1 polarization direction parallel to the trench in subduction zones, a phenomenon observed in other subduction zones. Therefore, when considering mantle peridotite regions rich in amphibole, the impact of amphibole on seismic anisotropy must be accounted for.
Full article
(This article belongs to the Special Issue Texture and Microstructural Analysis of Crystalline Solids, Volume II)
Open AccessArticle
Geochemical Signature and Risk Assessment of Potential Toxic Elements in Intensively Cultivated Soils of South-West Punjab, India
by
Umakant Chaudhari, Disha Kumari, Tanishka Tyagi, Sunil Mittal and Prafulla Kumar Sahoo
Minerals 2024, 14(6), 576; https://doi.org/10.3390/min14060576 - 30 May 2024
Abstract
Soil contamination with potentially toxic elements (PTEs) in the Malwa region belt of Punjab, India, can be a serious concern as a result of intensive agricultural practices and overuse of agrochemicals. The main objectives of the present study were to evaluate the spatial
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Soil contamination with potentially toxic elements (PTEs) in the Malwa region belt of Punjab, India, can be a serious concern as a result of intensive agricultural practices and overuse of agrochemicals. The main objectives of the present study were to evaluate the spatial distribution, geochemical signature, and contamination level/health risk of PTEs in 76 soil samples (0–10 cm) collected from the three districts viz. Muktar, Faridkot, and Moga of Punjab, India. The result shows that PTEs concentrations vary widely in the region, with Fe and Mn distribution patterns being mostly coherent with each other. When compared to the Indian natural soil background values, the average concentration of Pb and Zn were higher than the limit, only Pb exceeded the average values of the world background and upper continental crust (UCC). Spatial autocorrelation plotted with a local indicator of spatial association (LISA) in GeoDa software version 1.18 was used to identify hotspots. A positive spatial autocorrelation (>0.2) was indicated with Moran’s I values for Pb, V, Mn, Cu, and Cr, being highest for Pb. A principal component analysis (PCA) identified the major geo-chemical patterns of Fe-Al-V-Cr and TOC-Mn-Zn-HCO3−, which were positively loaded on PC1. This indicates that Fe/Al-oxyhydroxides and organic matter play a dominant role in controlling metal mobility in soils. This can be further substantiated with the Spearman’s rank correlation values. The contamination factor indicates that only Pb and Zn (15.7% and 3.9% samples, respectively) were under high risk. This could be due to the excessive application of chemical fertilizers. The large range of Cdeg values suggests that there are variations in the degree of soil pollution due to PTEs. A little over 3.9% of samples had significant contamination, compared to 72.3% of samples with low contamination and 23.6% of samples with moderate contamination. Human non-carcinogenic and carcinogenic risk levels were investigated. The HI values for adult ranged from 0.00 to 0.2, and values for children ranged from 0.009 to 1.2. These findings suggest that both children and adults are not at potential risk, except in a few locations. Overall, the results of this study provide the current baseline status of toxic elements in agricultural soil. This would be helpful for developing strategies for sustainable management of the soil resources in the region, as well as for future monitoring programs of the soil quality in the Malwa region as a whole, to track any changes in the contamination levels over time.
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(This article belongs to the Special Issue Heavy Metal and Rare Earth Element Pollution in Soil and Water: Sources, Geochemical Behaviors and Ecological Effects)
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40Ar/39Ar Dating and In Situ Trace Element Geochemistry of Quartz and Mica in the Weilasituo Deposit in Inner Mongolia, China: Implications for Li–Polymetallic Metallogenesis
by
Xue Wang, Ke-Yong Wang, Yang Gao, Jun-Chi Chen, Han-Wen Xue and Hao-Ming Li
Minerals 2024, 14(6), 575; https://doi.org/10.3390/min14060575 (registering DOI) - 30 May 2024
Abstract
The Weilasituo Li–polymetallic deposit, located on the western slope of the southern Great Xing’an Range in the eastern Central Asian Orogenic Belt, is hosted by quartz porphyry with crypto-explosive breccia-type Li mineralisation atop and vein-type Sn-Mo-W-Zn polymetallic mineralisation throughout the breccia pipe. This
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The Weilasituo Li–polymetallic deposit, located on the western slope of the southern Great Xing’an Range in the eastern Central Asian Orogenic Belt, is hosted by quartz porphyry with crypto-explosive breccia-type Li mineralisation atop and vein-type Sn-Mo-W-Zn polymetallic mineralisation throughout the breccia pipe. This study introduces new data on multistage quartz and mica in situ trace elements; the study was conducted using laser ablation inductively coupled plasma mass spectrometry and 40Ar/39Ar dating of zinnwaldite to delineate the metallogenic age and genesis of Li mineralisation. Zinnwaldite yields a plateau age of 132.45 ± 1.3 Ma (MSWD = 0.77), representing Early Cretaceous Li mineralisation. Throughout the magmatic–hydrothermal process, quartz trace elements showed Ge enrichment. Li, Al, and Ti contents decreased, with Al/Ti and Ge/Ti ratios increasing, indicating increased magmatic differentiation, slight acidification, and cooling. Mica’s rising Li, Rb, Cs, Mg, and Ti contents and Nb/Ta ratio, alongside its falling K/Rb ratio, indicate the magma’s ongoing crystallisation differentiation. Fractional crystallisation primarily enriched Li, Rb, and Cs in the late melt. Mica’s high Sc, V, and W contents indicate a high fO2 setting, with a slightly lower fO2 during zinnwaldite formation. Greisenisation observed Zn, Mg, and Fe influx from the host rock, broadening zinnwaldite distribution and forming minor Zn vein orebodies later. Late-stage fluorite precipitation highlights a rise in F levels, with fluid Sn and W levels tied to magma evolution and F content. In summary, the Weilasituo Li–polymetallic deposit was formed in an Early Cretaceous extensional environment and is closely related to a nearby highly differentiated Li-F granite. During magma differentiation, rare metal elements such as Li and Rb were enriched in residual melts. The decrease in temperature and the acidic environment led to the precipitation of Li-, Rb-, and W-bearing minerals, and the increased F content in the late stage led to Sn enrichment and mineralisation. Fluid metasomatism causes Zn, Mg, and Fe in the surrounding rock to enter the fluid, and Zn is enriched and mineralised in the later period.
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(This article belongs to the Special Issue Genesis and Metallogeny of Non-ferrous and Precious Metal Deposits, 2nd Edition)
Open AccessArticle
Peculiar Features of Lime-Treated Pyroclastic Soils through a Multi-Scale Experimental Investigation
by
Manuela Cecconi and Giacomo Russo
Minerals 2024, 14(6), 574; https://doi.org/10.3390/min14060574 - 30 May 2024
Abstract
Soil-improvement techniques with binders are used in several geotechnical engineering applications as a sustainable solution for the reuse of waste soils. Due to their inherent complexity and their mechanical behaviour, pyroclastic soils are generally considered waste geomaterials in their natural state. Lime treatment
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Soil-improvement techniques with binders are used in several geotechnical engineering applications as a sustainable solution for the reuse of waste soils. Due to their inherent complexity and their mechanical behaviour, pyroclastic soils are generally considered waste geomaterials in their natural state. Lime treatment of pyroclastic soils can be considered a viable solution for their reuse in geotechnical applications. In this paper, some peculiar features of the chemo-physical evolution and mechanical behaviour of lime-treated pyroclastic soils are evidenced through a multi-scale experimental investigation. While, for clayey soils, the fine fraction is mainly responsible for ion exchange and pozzolanic reactions induced by lime, for pyroclastic soils, pozzolanic reactions are dominant processes due to the low quantity of clay minerals along with the abundance of aluminates and silicates as the main constituents of their amorphous phase. The link between the phenomena detected at the microscale level, the mineralogical composition, and the macroscopic behaviour of two lime treated pyroclastic soils of different origin is explored through a multiscale approach.
Full article
(This article belongs to the Special Issue Chemo-Physical Evolution, Microstructural Modifications and Hydro-Mechanical Behaviour of Treated Soils of Different Mineralogical Composition)
Open AccessArticle
Zircon U–Pb Dating and Lu–Hf Isotopic Composition of Some Granite Intrusions in Northern and Central Portugal: Constraints on the Emplacement Age and Nature of the Source Rocks
by
Ana Gonçalves, Rui Teixeira, Helena Sant’Ovaia and Fernando Noronha
Minerals 2024, 14(6), 573; https://doi.org/10.3390/min14060573 - 30 May 2024
Abstract
Freixo de Numão (FNG) and Capinha (CG) granites are prominent intrusions in the Douro Group (northern Central Iberian Zone, CIZ) and Beiras Supergroup (southern CIZ) metasediments, respectively. U-Pb dating revealed crystallization ages of 306 ± 2 Ma for FNG and 301 ± 3
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Freixo de Numão (FNG) and Capinha (CG) granites are prominent intrusions in the Douro Group (northern Central Iberian Zone, CIZ) and Beiras Supergroup (southern CIZ) metasediments, respectively. U-Pb dating revealed crystallization ages of 306 ± 2 Ma for FNG and 301 ± 3 Ma for CG, whereas Lu–Hf systematics has shown ɛHft values ranging from −4.5 to +0.6 and from −5.5 to +0.3 in FNG and CG autocrysts, respectively, suggesting that they originate from heterogeneous crustal anatectic melts, but a direct mantle-derived material contribution can also be considered. The isotopic data of inherited zircon cores of both granites, with ɛHft values ranging from −16.8 to +8.4 in FNG, and from −19.4 to +10.1 in CG, are compatible with a derivation from heterogeneous Neoproterozoic metasedimentary sources, consisting of juvenile and recycled crustal materials, comparable to those of the wall rocks. However, the less evolved initial 176Hf/177Hf signature of magmatic zircons of both granites requires more immature metasediments/juvenile materials as main sources for the parental magmas. In fact, for FNG, the high Sr and Ba whole-rock content, and the upper Cambrian inheritance highlight the involvement of a metaigneous protolith in its genesis.
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(This article belongs to the Section Mineral Geochemistry and Geochronology)
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Zircon, Monazite SHRIMP U-Th-Pb and Quartz Oxygen Isotopic Results from the Higher Himalayan Crystallines (HHC) of the Sikkim Himalayas
by
Shashank Prabhamohan, Ian S. Williams and Sandeep Singh
Minerals 2024, 14(6), 572; https://doi.org/10.3390/min14060572 - 30 May 2024
Abstract
Migmatites and partial melts are exposed in both the lower and upper package of the Higher Himalayan Crystallines (HHC) thrust sheet within the Sikkim Himalayas. Zircon monazite and quartz oxygen isotopic ratios from Yumthang Valley, North Sikkim, and Rathong Chuu, West Sikkim, have
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Migmatites and partial melts are exposed in both the lower and upper package of the Higher Himalayan Crystallines (HHC) thrust sheet within the Sikkim Himalayas. Zircon monazite and quartz oxygen isotopic ratios from Yumthang Valley, North Sikkim, and Rathong Chuu, West Sikkim, have been used to identify their sources and equilibrium conditions. Monazites show homogeneous growth, whereas zircons show growth rings. U-Th-Pb data on monazite only indicate the latest metamorphic event. However, zircons show metamorphic rim growth between 36 and 24 Ma over their detrital core with trailing growth from 22 Ma to 15 Ma. Pervasive fluids have been interpreted in coeval development during metamorphism, as shown by monazite and zircon c. 30 Ma. The Th/U ratio of zircon is higher and variable with weak residual zoning in the samples from higher elevations. Quartz–metamorphic zircon oxygen fractionation suggests Teq > 600 °C, while quartz–monazite fractionation shows the same or lower temperatures. Multiple sources of melts in the HHC (even along a single valley) have been observed by δ18O of 7‰ to 10‰ in zircon and 5‰ to 9‰ in monazite. Zircon and monazite generated in the same rock have similar δ18O values. Monazite grown ~20 Ma in the lower elevation sample had a low δ18O, suggesting interaction with an external fluid.
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(This article belongs to the Special Issue Advances in Mantle–Crust Interactions for Petrogenesis and Ore-Forming Processes)
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Open AccessReview
Advanced Processing Techniques and Impurity Management for High-Purity Quartz in Diverse Industrial Applications
by
Hailin Long, Deqing Zhu, Jian Pan, Siwei Li, Congcong Yang and Zhengqi Guo
Minerals 2024, 14(6), 571; https://doi.org/10.3390/min14060571 - 30 May 2024
Abstract
While numerous studies have explored the mineralogical characteristics and purification techniques of high-purity quartz (HPQ), discussions on impurity control during various purification processes and their applications in photovoltaics, electronics, and optics remain limited. This review delves into the adverse effects of impurities such
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While numerous studies have explored the mineralogical characteristics and purification techniques of high-purity quartz (HPQ), discussions on impurity control during various purification processes and their applications in photovoltaics, electronics, and optics remain limited. This review delves into the adverse effects of impurities such as aluminum, iron, and sodium in the manufacturing processes of these industries, emphasizing their critical role as these impurities can degrade material performance. This paper focuses on analyzing the types of impurities found in quartz and evaluates existing purification technologies such as acid washing, ultrasonic acid washing, chlorination roasting, and calcination quenching. It highlights the limitations of current technologies in processing quartz ore and discusses the advantages of different impurity types under various technological treatments. Moreover, it explores the environmental and economic impacts of these high-purity processes, underlining the necessity for more environmentally friendly and cost-effective purification techniques. The purpose of this review is to provide a comprehensive technical and strategic framework for the use of high-purity quartz in high-tech applications, supporting future research and industrial applications in this critical material field.
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(This article belongs to the Special Issue Advances in Mineral Processing and Extractive Metallurgy of Base and Precious Metals)
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Microstructure Evolution Law of Ionic Rare Earth at Different Depths in In Situ Leaching Mine Site
by
Zhongqun Guo, Haoxuan Wang, Qiqi Liu, Feiyue Luo and Yanshuo Liu
Minerals 2024, 14(6), 570; https://doi.org/10.3390/min14060570 - 29 May 2024
Abstract
Due to the inhomogeneity and anisotropy of mine rock bodies, ionic rare earth ore bodies exhibit varying pore structures at different depths. This research focuses on an ionic rare earth mine in Fujian Province, where in situ ore samples rather than remodeled soil
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Due to the inhomogeneity and anisotropy of mine rock bodies, ionic rare earth ore bodies exhibit varying pore structures at different depths. This research focuses on an ionic rare earth mine in Fujian Province, where in situ ore samples rather than remodeled soil samples were studied. Samples from the fully weathered layer at depths of 1 m, 12 m, and 21 m, both before and after leaching, were collected for onsite analysis. Microscopic pore characteristics were evaluated using scanning electron microscopy, and digital image processing was utilized to study the evolution of the pore scale, distribution, and shape in rare earth ore samples at various depths pre- and post-leaching. The results indicate an increase in the ore body’s porosity with the depth of the ore samples both before and after leaching. The variation in pore scale is predominantly dictated by the ratio of macropore and large pores. Pre-leaching, the middle ore sample showcased the highest uniformity, with the upper part being the most irregular. Post-leaching, the highest uniformity was observed in the lower ore samples, with the upper part remaining irregular. Pre-leaching, as depth increased, the pore distribution in ore samples became more dispersed, with decreasing orderliness. Post-leaching, the orderliness was most improved in upper ore samples, while middle ore samples became the least orderly. Additionally, before leaching, pore-shape roughness increased with depth; after leaching, the pore shape became more rounded as depth increased, simplifying the pore-shape structure of the ore samples both before and after leaching.
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(This article belongs to the Special Issue Green and Efficient Recovery/Extraction of Rare Earth Resources)
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Zircon U-Pb Geochronology, Geochemistry, and Sr-Nd-Hf Isotopic Composition of Ben Giang-Que Son Complex in the Southern Truong Son Belt: Implications for Permian–Triassic Tectonic Evolution
by
Thuy Thi Bich Nguyen, Pham Trung Hieu, Qian Xin, Bui The Anh, Nguyen Thi Xuan, Pham Minh and Ho Thi Thu
Minerals 2024, 14(6), 569; https://doi.org/10.3390/min14060569 - 29 May 2024
Abstract
The magmatic rocks of the Ben Giang-Que Son complex exposed in the southern part of the Truong Son belt have petrographic compositions including gabbro, gabbrodiorite, granodiorite, and granite. Geochemically, the magmatic rocks are of subalkaline affinity and belong to the high-K calc-alkaline series.
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The magmatic rocks of the Ben Giang-Que Son complex exposed in the southern part of the Truong Son belt have petrographic compositions including gabbro, gabbrodiorite, granodiorite, and granite. Geochemically, the magmatic rocks are of subalkaline affinity and belong to the high-K calc-alkaline series. All analyzed samples contain hornblende and biotite as mafic minerals and are defined as metaluminous with a aluminum saturation index of <1.1. Chondrite-normalized rare earth element diagrams are characterized by fractionation between light and heavy rare earth elements and show small to moderate negative Eu anomalies (Eu/Eu* = 0.81–0.44). Primitive mantle-normalized trace element patterns exhibit enrichment in LILEs such as Rb, K, U, and especially Pb and depletion of HFSEs (Nb, Ta, and Ti), indicating arc-magma. The BG-QS gabbro and gabbrodiorite have low Cr, Co, and Ni and display enrichment in 87Sr/86Sr (0.7084 to 0.7147), ꜪNd(t) (−0.5 to −1.9), and positive ꜪHf(t) (+2.4 to 4.5), suggesting generation from the enriched mantle source. The BG-QS diorite and granodiorite contain small mafic enclaves, have a wide range of SiO2 contents and enrichment in Sr-Nd isotopes (87Sr/86Sr = 0.7109–0.7178; ꜪNd(t) = −3.3 to −3.7), and display high Mg# (43–51). All these features indicate that they were formed by the mixing of magmas, which originated from an enriched mantle source and the pre-existing juvenile mafic lower crust. The whole-rock Nd and zircon Hf model ages are of 1160–760 Ma. The Ben Giang-Que Son complex yields LA-ICP-MS zircon U-Pb ages of 285 ± 3.1 and 278 ± 3.5 Ma that corresponds to the Cisuralian epoch (early Permian), which is linked to the subduction and amalgamation of the Indochina and South China blocks due to the closing a branch of the Paleotethys along the Song Ma suture.
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(This article belongs to the Special Issue Petrogenesis, Magmatism and Geodynamics of Orogenic Belts)
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The Chemistry and Mineralogy (CheMin) X-ray Diffractometer on the MSL Curiosity Rover: A Decade of Mineralogy from Gale Crater, Mars
by
David Blake, Valerie Tu, Thomas Bristow, Elizabeth Rampe, David Vaniman, Steve Chipera, Philippe Sarrazin, Richard Morris, Shaunna Morrison, Albert Yen, Robert Downs, Robert Hazen, Allan Treiman, Douglas Ming, Gordon Downs, Cherie Achilles, Nicholas Castle, Tanya Peretyazhko, David De Marais, Patricia Craig, Barbara Lafuente, Benjamin Tutolo, Elisabeth Hausrath, Sarah Simpson, Richard Walroth, Michael Thorpe, Johannes Meusburger, Aditi Pandey, Marc Gailhanou, Przemyslaw Dera, Jeffrey Berger, Lucy Thompson, Ralf Gellert, Amy McAdam, Catherine O’Connell-Cooper, Brad Sutter, John Michael Morookian, Abigail Fraeman, John Grotzinger, Kirsten Siebach, Soren Madsen and Ashwin Vasavadaadd
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Minerals 2024, 14(6), 568; https://doi.org/10.3390/min14060568 - 29 May 2024
Abstract
For more than a decade, the CheMin X-ray diffraction instrument on the Mars Science Laboratory rover, Curiosity, has been returning definitive and quantitative mineralogical and mineral–chemistry data from ~3.5-billion-year-old (Ga) sediments in Gale crater, Mars. To date, 40 drilled rock samples and
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For more than a decade, the CheMin X-ray diffraction instrument on the Mars Science Laboratory rover, Curiosity, has been returning definitive and quantitative mineralogical and mineral–chemistry data from ~3.5-billion-year-old (Ga) sediments in Gale crater, Mars. To date, 40 drilled rock samples and three scooped soil samples have been analyzed during the rover’s 30+ km transit. These samples document the mineralogy of over 800 m of flat-lying fluvial, lacustrine, and aeolian sedimentary rocks that comprise the lower strata of the central mound of Gale crater (Aeolis Mons, informally known as Mt. Sharp) and the surrounding plains (Aeolis Palus, informally known as the Bradbury Rise). The principal mineralogy of the sedimentary rocks is of basaltic composition, with evidence of post-depositional diagenetic overprinting. The rocks in many cases preserve much of their primary mineralogy and sedimentary features, suggesting that they were never strongly heated or deformed. Using aeolian soil composition as a proxy for the composition of the deposited and lithified sediment, it appears that, in many cases, the diagenetic changes observed are principally isochemical. Exceptions to this trend include secondary nodules, calcium sulfate veining, and rare Si-rich alteration halos. A surprising and yet poorly understood observation is that nearly all of the ~3.5 Ga sedimentary rocks analyzed to date contain 15–70 wt.% of X-ray amorphous material. Overall, this >800 m section of sedimentary rock explored in lower Mt. Sharp documents a perennial shallow lake environment grading upward into alternating lacustrine/fluvial and aeolian environments, many of which would have been habitable to microbial life.
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(This article belongs to the Special Issue Mineralogy and Geochemistry of Mars: Everything You Need to Know about the Red Planet)
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Soil Geochemistry Combined with Particulate Gold Microchemistry Provides Evidence of Eluvial Gold Genesis and Anthropogenic Hg Use in Eastern Cameroon Goldfields
by
Akumbom Vishiti, Cheo Emmanuel Suh, Ralain Bryan Ngatcha, Erik B. Melchiorre, Elisha Mutum Shemang, Benjamin Odey Omang, Terence Cho Ngang, Fernando Castro Valdez and Sharila Gillian Sekem
Minerals 2024, 14(6), 567; https://doi.org/10.3390/min14060567 - 29 May 2024
Abstract
The identification of trace element anomalies in soils has been proven to assist semi-mechanized small-scale gold operations. This study employs soil geochemistry combined with the microchemical signature of particulate gold from the Batouri goldfield to (1) vector possible gold-endowed lithologies introducing particulate gold
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The identification of trace element anomalies in soils has been proven to assist semi-mechanized small-scale gold operations. This study employs soil geochemistry combined with the microchemical signature of particulate gold from the Batouri goldfield to (1) vector possible gold-endowed lithologies introducing particulate gold into the overlying regolith, and (2) assess anthropogenic Hg used in purification of both primary and alluvial/eluvial gold by artisans. The soil geochemistry shows irregularly distributed anomalies of elevated Cu especially in the saprolite soil layer. Whereas in the lateritic soil layer, a Au-Ag-Hg metal association is reported for the first time in this gold district and could be linked to anthropogenic Hg used in gold recovery. Particulate gold recovered from the soil varies in shape from euhedral and irregular to sub-rounded, indicating a proximal lode source. The gold grains range in size from nano-particles to >300 µm and are Au-Ag alloys. The gold particles reveal inclusions such as quartz, silicate, zircon and ilmenite suggesting that the grains were dislodged from quartz veins within the granitic basement. Systematic variation in the microchemical signature of the gold grains is suggestive of spatial and temporal evolution of the mineralizing fluid. These results are consistent with investigations from similar geologic settings worldwide and validate the combined utility of gold fingerprinting and pathfinder elements in soil to examine deposit genesis in other gold districts globally.
Full article
(This article belongs to the Special Issue Structure and Origin of Gold Mineralization: From Primary to Placer Gold Deposits)
Open AccessArticle
Assessing the Performance of CO2-Mineralized Underground Backfilling Materials through the Variation Characteristics of Infrared Radiation Temperature Index
by
Guanghui Cao, Liqiang Ma, Arienkhe Endurance Osemudiamhen, Ichhuy Ngo, Qiangqiang Gao, Kunpeng Yu and Zezhou Guo
Minerals 2024, 14(6), 566; https://doi.org/10.3390/min14060566 - 29 May 2024
Abstract
The utilization of CO2 mineralization fly ash (F) and coal gangue (G) technology is proposed in this research work to prepare underground backfilling materials. The test process can be divided into pre-treatment and post-treatment stages. In the pre-treatment stage, a sealed stirring
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The utilization of CO2 mineralization fly ash (F) and coal gangue (G) technology is proposed in this research work to prepare underground backfilling materials. The test process can be divided into pre-treatment and post-treatment stages. In the pre-treatment stage, a sealed stirring vessel is used to conduct CO2 wet mineralization. The ratios of F and G were selected as follows: 20%:60% (F2G6), 30%:50% (F3G5), 40%:40% (F4G4), 50%:30% (F5G3), and 60%:20% (F6G2). The ratios were prepared into Φ50 mm × 100 mm cylindrical samples, with curing durations of 3 d, 7 d, 14 d, and 28 d. In the post-processing stage, the SANS microcomputer-controlled electronic universal testing machine and FLIR A615 infrared thermal imager were used to carry out uniaxial loading and temperature detection, respectively. The unconfined compressive strength (UCS), X-ray diffraction (XRD), average infrared radiation temperature (AIRT), variance of original infrared image temperature (VOIIT), and variance of successive minus infrared image temperature (VSMIT) of the samples were compared and analyzed. The results indicated that when curing reaches 14 d, the strength approaches its peak, with minimal changes in strength over a delayed period; furthermore, as the ratio of F to G continues to increase, the mineralization effect gradually strengthens, reaching its optimum level at a ratio of 5:3. However, when the ratio exceeds 5:3, signs of deteriorating mineralization effect start to appear. During the loading process, the AIRT of the mineralized samples showed a continuous increase, but the VOIIT and VSMIT of the mineralized sample both exhibited significant fluctuations or rapid increases during damage rupture. Moreover, the rise in the AIRT value was found to be linked to the increase in the ratio of F to G. This indicates that F has a higher thermal–mechanical conversion efficiency compared to G, so the temperature change will be greater during the loading process. The drastic changes in the VOIIT and VSMIT indicate that they can be used as sensitive response indicators for sample rupture, and can predict and warn of damage rupture in mineralized samples. Research work can provide practical guidance and reference for underground backfilling of CO2 mineralization industrial waste.
Full article
(This article belongs to the Section Mineral Processing and Extractive Metallurgy)
Open AccessArticle
Petrogenesis and Metallogenesis of Late Cretaceous Adakites in the Nuri Large Cu-W-Mo Deposit, Tibet, China: Constraints from Geochronology, Geochemistry, and Hf Isotopes
by
Zhishan Wu, Yiyun Wang, Hongzhao Shi, Bin Chen, Yong Huang, Qingan Du, Wenqing Chen, Liwei Tang and Yun Bai
Minerals 2024, 14(6), 565; https://doi.org/10.3390/min14060565 - 29 May 2024
Abstract
The Gangdese metallogenic belt in Tibet is an important polymetallic metallogenic belt formed during the subduction of the Neo-Tethys Ocean and subsequent India–Asia collision. Adakitic rocks are widely distributed in this belt and are considered to be closely related to porphyry–skarn Cu-Mo polymetallic
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The Gangdese metallogenic belt in Tibet is an important polymetallic metallogenic belt formed during the subduction of the Neo-Tethys Ocean and subsequent India–Asia collision. Adakitic rocks are widely distributed in this belt and are considered to be closely related to porphyry–skarn Cu-Mo polymetallic mineralization. However, the petrogenesis and geodynamic setting of the Late Cretaceous adakites in the Gangdese belt remain controversial. In this study, we focus on the quartz diorite in the Nuri Cu-W-Mo deposit along the southern margin of the eastern Gangdese belt. LA-ICP-MS zircon U-Pb dating yields a Late Cretaceous age of 93.6 ± 0.4 Ma for the quartz diorite. Whole-rock geochemistry shows that the quartz diorite possesses typical adakitic signatures, with high SiO2, Al2O3, and Sr contents, but low Y and Yb contents. The relatively low K2O content and high MgO, Cr, and Ni contents, as well as the positive zircon εHf(t) values (+6.58 to +14.52), suggest that the adakites were derived from the partial melting of the subducted Neo-Tethys oceanic slab, with subsequent interaction with the overlying mantle wedge. The Late Cretaceous magmatic flare-up and coeval high-temperature granulite-facies metamorphism in the Gangdese belt were likely triggered by Neo-Tethys mid-ocean ridge subduction. The widespread occurrence of Late Cretaceous adakitic intrusions and associated Cu mineralization in the Nuri ore district indicate a strong tectono-magmatic-metallogenic event related to the Neo-Tethys subduction during this period. This study provides new insights into the petrogenesis and geodynamic setting of the Late Cretaceous adakites in the Gangdese belt, and has important implications for Cu polymetallic deposit exploration in this region.
Full article
(This article belongs to the Special Issue Indicator Minerals, Vectoring and Fertility Tools for the Exploration of Porphyry Cu (Mo ± Au) Systems)
Open AccessArticle
Genesis of Gypsum/Anhydrite in the World-Class Jinding Zn-Pb Deposit, SW China: Constraints from Field Mapping, Petrography, and S-O-Sr Isotope Geochemistry
by
Gang Huang, Yu-Cai Song, Liang-Liang Zhuang, Chuan-Dong Xue, Li-Dan Tian and Wei Wu
Minerals 2024, 14(6), 564; https://doi.org/10.3390/min14060564 - 29 May 2024
Abstract
The world-class Jinding deposit in SW China has ~15 Mt of Zn and Pb metals combined, in an evaporite dome containing amounts of gypsum/anhydrite. These gypsum and anhydrite are mainly located in limestone breccias (Member I), gypsum-bearing complexes (Member III), and red mélange,
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The world-class Jinding deposit in SW China has ~15 Mt of Zn and Pb metals combined, in an evaporite dome containing amounts of gypsum/anhydrite. These gypsum and anhydrite are mainly located in limestone breccias (Member I), gypsum-bearing complexes (Member III), and red mélange, with some occurring as veins in clast-free sandstone (Member IV) and as fractures/vugs of host rock. The gypsum/anhydrite and dome genesis remain equivocal. The gypsum in limestone breccias and in red mélange with flow texture contains numerous Late Triassic Sanhedong limestone fragments. The δ34S (14.1%–17%), δ18O (9.7%–14.6%), and 87Sr/86Sr ratios (0.706913–0.708711) of these gypsum are close to the S-O-Sr isotopes of the Upper Triassic Sanhedong Formation anhydrite in the Lanping Basin (δ34S = 15.2%–15.9%, δ18O = 10.9%–13.1%, 87Sr/86Sr = 0.707541–0.707967), and are inconsistent with the Paleocene Yunlong Formation gypsum in the Lanping Basin (87Sr/86Sr = 0.709406–0.709845), indicating that these gypsum were derived from the Upper Triassic Sanhedong Formation evaporite but not from the Paleocene Yunlong Formation, and formed as a result of evaporite diapirism. The δ34S (14.3%–14.5%), δ18O (10.1%–10.3%), and 87Sr/86Sr ratios (0.709503–0.709725) of gypsum as gypsum–sand mixtures in gypsum-bearing complexes are similar to the 87Sr/86Sr ratios of gypsum in the Yunlong Formation of the Lanping Basin and Cenozoic basins in the northern part of the Himalayan–Tibetan orogen, suggesting that the material source of this gypsum was derived from the Yunlong Formation, and formed as a result of gypsum–sand diapirism. The gypsum veins in clast-free pillow-shaped mineralized sandstone and the gypsum in host rock fractures and vugs formed after the supergene minerals such as smithsonite. The δ34S (−16.3%~−12.7%) and δ18O (−9.8%~−4.7%) of this gypsum indicate that the gypsum is of supergene origin with sulfate derived from the reoxidation of reduced sulfur. We confirmed that the Jinding dome is genetically related to diapir of the Late-Triassic Sanhedong Formation evaporite. Clast-free sandstone and gypsum-bearing complexes in the dome were produced by diapir of the Paleocene Yunlong Formation unconsolidated gypsum–sand mixtures.
Full article
(This article belongs to the Special Issue Ag-Pb-Zn Deposits: Geology and Geochemistry)
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Open AccessArticle
DIGIT: An In Situ Experiment for Studying the Diffusion of Water and Solutes under Thermal Gradient in the Toarcian Clay Rock at the Tournemire Underground Research Laboratory: Part 1—Goals, Scoping Calculations, Installation and First Results under Unheated Conditions
by
Maïwenn Humbezi Desfeux, Manuel Marcoux, Jean-Michel Matray, Josselin Gorny, Philipp Schädle and Guillaume Pochet
Minerals 2024, 14(6), 563; https://doi.org/10.3390/min14060563 - 29 May 2024
Abstract
The DIGIT experiment was launched at the Tournemire Underground Research Laboratory URL with the aim of determining the effects of temperature on the transfer of analogues of most mobile radionuclides (i.e., 36Cl, 129I and 79Se) in the Toarcian clay rock,
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The DIGIT experiment was launched at the Tournemire Underground Research Laboratory URL with the aim of determining the effects of temperature on the transfer of analogues of most mobile radionuclides (i.e., 36Cl, 129I and 79Se) in the Toarcian clay rock, the properties of which are close to host rocks being considered for future deep geological disposal of high-level (HL) radioactive wastes. The experimental principle involves the monitoring of an exchange between a test water traced with stable halides and deuterium at constant concentration and the porewater of the Toarcian clay rock submitted to various temperatures. This experiment seeks to partially address questions regarding the potential spread of contaminants during the thermal phase of High Level Waste (HLW) waste packages. Specifically, the in situ experiment aims to evaluate the role of scale effects and thermodiffusion, a process that combines Fick’s law and the Soret effect, in the transfer of radionuclides. This paper presents the first steps of the study, including the scoping calculations, the experimental set-up and the first results obtained during the unheated phase. The study started with the acquisition of the initial parameters, including the rock thermal properties, the concentrations of the four tracers (chloride, bromide, iodide and deuterium) naturally present in the clay porewater and their diffusive transport parameters by using four diffusion exchange techniques (phase 0). A model coupling heat and mass transfers was then developed using Comsol Multiphysics®, integrating data acquired so far with existing literature data. A test water with a tracer concentration around 1000 times higher than those in the pore water was proposed with a temperature imposed at the test section wall of 70 °C. A large test zone of 50 cm height and 1 m in diameter and installed in a 3 m deep vertical well located in a sound zone at the URL was then proposed. The installation of the experiments required the realization of one shaft and of nine peripheral boreholes for the monitoring of temperature, water pressure and deformation. The experiment started with phase 1, involving a traced, unheated water start-up for a period of 5 months. Then, a core sampling was conducted in the emptied well, and the same diffusion exchange techniques were applied. The results of anionic tracers were compared to simulations based on initial parameters (phase 0), revealing that tracer penetration at the end of phase 1 exceeded simulated values by approximately 2 cm. This result is interpreted as an increase in the accessible porosity to tracers, possibly due to the excavation damaged zone. Future simulations should incorporate these adjusted diffusive transport parameters. Following phase 1, the heating system was activated, applying a temperature of 70 °C to the test zone. New data will enable the comparison of tracer penetration and assess the actual impact of temperature on tracer transfer.
Full article
(This article belongs to the Special Issue Implications of THMC Processes on Long-Term Safety of Geological Disposal of Radioactive Waste)
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Open AccessArticle
Determination of the Formation Time of the Present Tectonic Framework in the Dabie Orogen, Eastern China: Zircon U-Pb Geochronology and Al-in-Hornblende Geobarometer
by
Yongsheng Wang, Juanhao Yang, Qiao Bai, Xu Zhang and Zhensheng Li
Minerals 2024, 14(6), 562; https://doi.org/10.3390/min14060562 - 29 May 2024
Abstract
The Dabie–Sulu Orogen hosts the largest province of ultrahigh-pressure (UHP) rocks in the world. The post-collisional extension eroded and transported volumes of rocks from the Dabie Orogen to adjacent basins, causing a lack of information about the orogen and thus obstructing our understanding
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The Dabie–Sulu Orogen hosts the largest province of ultrahigh-pressure (UHP) rocks in the world. The post-collisional extension eroded and transported volumes of rocks from the Dabie Orogen to adjacent basins, causing a lack of information about the orogen and thus obstructing our understanding of the exhumation process of UHP rocks. In addition, the mechanisms that triggered the post-collisional extension and affected the petrological-tectonic units of the orogen are still unclear. This study is focused on the time in which the present tectonic framework in the Dabie Orogen took place, selecting Early Cretaceous plutons in the eastern part of the orogen and carrying out detailed zircon LA-ICP-MS U-Pb dating and crystallization depth calculation. The zircon dating results show that the emplacement time of the Meichuan and Luannitan plutons and the Penghe superunit of the Zhubuyuan pluton are all ~128 Ma, while the Huangbai superunit of the Zhubuyuan pluton and the Longmianzhai pluton formed at ~125 Ma. The emplacement time and later anatexis of the Baimajian pluton occurred at ~128 and ~122 Ma, respectively. The results of the Al-in-hornblende geobarometer show that plutons of ~128 Ma have a similar crystallization depth, while plutons of ~125 Ma range from 7.6 to 9.5 km. The Baimajian pluton has a greater crystallization depth. Combined with the existing achievements, a conclusion can be drawn that the present tectonic framework of the Dabie Orogen began to form from ~128 Ma.
Full article
(This article belongs to the Special Issue Tectonic Evolution and Mineralization of the Dabie Orogen)
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Open AccessArticle
Timing and Tectonic Implications of the Development of the Orosirian Qianlishan Ductile Shear Zones in the Khondalite Belt, North China Craton
by
Hengzhong Qiao, Miao Liu and Chencheng Dai
Minerals 2024, 14(6), 561; https://doi.org/10.3390/min14060561 - 29 May 2024
Abstract
Orogen-parallel ductile shear zones are conspicuous structures in the Khondalite Belt, but the timing of shearing remains poorly understood. Here, we present field-based structural and zircon U-Pb geochronological studies on the newly discovered Qianlishan ductile shear zones (QDSZ) in the Khondalite Belt. Our
[...] Read more.
Orogen-parallel ductile shear zones are conspicuous structures in the Khondalite Belt, but the timing of shearing remains poorly understood. Here, we present field-based structural and zircon U-Pb geochronological studies on the newly discovered Qianlishan ductile shear zones (QDSZ) in the Khondalite Belt. Our results show that the nearly E-W-trending QDSZ are characterized by steeply S(SW)-dipping mylonitic foliations and mainly display a top-to-N(NE) sense of shearing. Two pre-kinematic intrusions yielded zircon crystallization ages of 2055 ± 17 Ma and 1947 ± 9 Ma, providing the maximum age limit for the QDSZ. Additionally, zircon overgrowth rims from three high-temperature mylonites gave metamorphic ages of 1902 ± 8 Ma, 1902 ± 26 Ma and 1884 ± 12 Ma, interpreted to record the timing of development of the QDSZ. Integrated with previous studies, we propose that the Qianlishan Complex suffered three phases of Orosirian deformation (D1–D3), of which the D3 deformation led to the development of the QDSZ. Deformation events D1, D2 and D3 are considered to have occurred at ca. 1.97–1.93 Ga, 1.93–1.90 Ga and 1.90–1.82 Ga, respectively. These events document that the Khondalite Belt underwent a protracted (>100 Myr) orogenic history in response to the collision between the Yinshan and Ordos blocks.
Full article
(This article belongs to the Special Issue Formation and Evolution of the Continental Crust in North China Craton during Precambrian)
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